Glycerol → 1160173-26-1

HRID 258280

反応式

HRID 258280 の反応式
[CH3:1][C@H:2]1[CH2:8][C:6](=[O:7])[C@H:5]([CH:9]([CH3:11])[CH3:10])[CH2:4][CH2:3]1.[OH:12][CH2:13][CH:14]([CH2:16]O)[OH:15].S([O-])(O)(=O)=O.[K+].O>C1(C)C=CC=CC=1>[CH3:1][C@H:2]1[CH2:8][C:6]2([O:15][CH:14]([CH2:13][OH:12])[CH2:16][O:7]2)[C@H:5]([CH:9]([CH3:11])[CH3:10])[CH2:4][CH2:3]1

参加物

6

反応物 4

HCID 753GlycerolHCID 962WaterHCID 26447MenthoneHCID 516920Potassium bisulfate

生成物 1

HCID 99646061160173-26-1

試薬・触媒・溶媒 1

HCID 1140Toluene溶媒

実験手順

In a 2 l three-necked flask there are introduced 308 g of 1-menthone (2 mol), 276 g of glycerol (3 mol) and 5 g of potassium hydrogen sulphate in toluene. This mixture is refluxed in a water separator. After 7 hours, 42 g of water have separated. The mixture is neutralised and distilled.

後処理

  1. custom42 g of water have separated
  2. distillationdistilled

出典と根拠

ORDレコード
ord-5839718a228d4b68a1e5eee670bc279b
出典データセット
uspto-grants-1993_11
特許番号
US05266592

関連ノート

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