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Ethanol → HCID 131710840、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Ethanol | HCID 702 | — |
| 反応物 | N-ethyl-3-methylaniline | HCID 7603 | — |
| 反応物 | Sodium Bicarbonate | HCID 516892 | — |
| 反応物 | 1-Bromo-2-(2-ethoxyethoxy)ethane | HCID 7015324 | — |
| 溶媒 | Water | HCID 962 | — |
| 生成物 | HCID 131710840 | HCID 131710840 | — |
反応手順
A mixture of 67.5 g(0.5 mole) of N-ethyl-3-methyl-aniline, 98.5 g (0.5 mole) of [β-(β-ethoxy)-ethoxy]ethyl bromide, 44.1 g (0.55 mole) of sodium bicarbonate, 5.50 ml of ethanol and 145 ml of water was refluxed for 80 hours. Ethanol was removed by distillation and the oil layer was extracted with ether. The extract was dried with potassium carbonate and then ether was removed, followed by distillation of the residue oil under reduced pressure.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04035188 |
| 出典データセット | uspto-grants-1977_07 |
| ORD ID | ord-a3059631fdba4057814c471ea83120ab |
| 出典メモ | uspto-grants-1977_07 |