Butyric Acid → Heptafluorobutyric acid

HRID 259473

反応式

HRID 259473 の反応式
[F:1][C:2]([F:13])([C:9]([F:12])([F:11])[F:10])[C:3]([F:8])([F:7])[C:4]([F:6])=[O:5].C(O)(=[O:18])CCC.C(OC(=O)CCC)(=O)CCC>>[F:10][C:9]([F:12])([F:11])[C:2]([F:13])([F:1])[C:3]([F:8])([F:7])[C:4]([OH:18])=[O:5].[C:4]([F:6])(=[O:5])[CH2:3][CH2:2][CH3:9]

参加物

5

実験手順

The following run illustrates the metathetical reaction of impure heptafluorobutyryl fluoride with butyric acid in the presence of butyric anhydride to give heptafluorobutyric acid and butyryl fluoride and the recovery of products from the reaction mixture by fractional distillation.

出典と根拠

ORDレコード
ord-f0fd27ea775447efb4ba9fb622217ab9
出典データセット
uspto-grants-1977_07
特許番号
US04038310

関連ノート

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