Benzene → Isobutylidenebenzhydrylamine
反応式
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[CH:6]([NH2:19])([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C1C=CC=CC=1>O>[CH:1](=[N:19][CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH:2]([CH3:4])[CH3:3]参加物
5
実験手順
14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.
後処理
- temperatureThe cloudy mixture was heated
- temperatureOn cooling the solution
- filtrationwas filtered
- customto remove a small amount of solid
- customevaporated
出典と根拠
- ORDレコード
- ord-c6b653a08d6e4a9db8afca08018af3b1
- 出典データセット
- uspto-grants-1979_04
- 特許番号
- US04147780
反応ノート
読み込み中…