Benzene → Isobutylidenebenzhydrylamine

HRID 25972

反応式

HRID 25972 の反応式
[CH:1](=O)[CH:2]([CH3:4])[CH3:3].[CH:6]([NH2:19])([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1.C1C=CC=CC=1>O>[CH:1](=[N:19][CH:6]([C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][CH:8]=1)[C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[CH:2]([CH3:4])[CH3:3]

参加物

5

反応物 3

HCID 241BenzeneHCID 6561IsobutyraldehydeHCID 7036Benzhydrylamine

生成物 1

HCID 10657527Isobutylidenebenzhydrylamine

試薬・触媒・溶媒 1

HCID 962Water溶媒

実験手順

14.4 parts of isobutyraldehyde was added to 36.6 parts of benzhydrylamine in 100 parts of dry benzene at room temperature with stirring. The cloudy mixture was heated to reflux with water-separation for 4 hours. On cooling the solution was filtered to remove a small amount of solid and evaporated to give isobutylidenebenzhydrylamine.

後処理

  1. temperatureThe cloudy mixture was heated
  2. temperatureOn cooling the solution
  3. filtrationwas filtered
  4. customto remove a small amount of solid
  5. customevaporated

出典と根拠

ORDレコード
ord-c6b653a08d6e4a9db8afca08018af3b1
出典データセット
uspto-grants-1979_04
特許番号
US04147780

関連ノート

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