Saccharin → 1,2,3,4-Tetrahydroquinoline

HRID 259794

反応式

HRID 259794 の反応式
S1(C2C(=CC=CC=2)C(=O)[NH:4]1)(=O)=O.[CH3:13]/[C:14](/O)=[CH:15]/[C:16]([CH3:18])=O.[CH3:20]/[C:21](/O)=[CH:22]/[C:23](C)=O.C/C(/O)=C/C(C)=O.[Fe]>C(OCCCO)(=O)C(C)=C.C1C=C2C(C=C(C([O-])=O)C=C2)=CC=1.C1C=C2C(C=C(C([O-])=O)C=C2)=CC=1.[Co+2]>[NH:4]1[C:18]2[C:16](=[CH:20][CH:21]=[CH:22][CH:23]=2)[CH2:15][CH2:14][CH2:13]1

参加物

5

反応物 2

HCID 5143SaccharinHCID 11110968Iron (III) acetylacetonate

生成物 1

HCID 694601,2,3,4-Tetrahydroquinoline

試薬・触媒・溶媒 2

HCID 14048876Cobaltous 2-naphthenic acid触媒HCID 176943-Hydroxypropyl methacrylate溶媒3 回

実験手順

An adhesive formulation prepared and tested as in Example 1 containing hydroxypropyl methacrylate (8.15 g), saccharin (0.5 g), 0.1% cobalt naphthenate in hydroxypropyl methacrylate (1 g), 0.1% iron (III) acetylacetonate in hydroxypropyl methacrylate (0.25 g) and 1,2,3,4 tetrahydroquinoline (0.5 g) gave bond strengths of 3.3 N/mm2 after 24 hours following air activation for 5 minutes.

後処理

  1. customAn adhesive formulation prepared

出典と根拠

ORDレコード
ord-fd1017a35d074823bb58e407d7e7711c
出典データセット
uspto-grants-1996_06
特許番号
US05523347

関連ノート

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