化工社化工社 化学情報印刷レポート · 研究参考用
3-Chloropropionyl chloride → 3-Chloro-1-(2-oxo-1,2,2a,3,4,5-hexahydrobenz[cd]indol-6-yl)-1-propanone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 3-Chloropropionyl chloride | HCID 69364 | — |
| 反応物 | 2a,3,4,5-Tetrahydrobenzo[cd]indol-2(1H)-one | HCID 599375 | — |
| 生成物 | 3-Chloro-1-(2-oxo-1,2,2a,3,4,5-hexahydrobenz[cd]indol-6-yl)-1-propanone | HCID 15296944 | — |
反応手順
Using 2a,3,4,5-tetrahydrobenz[cd]indol-2(1H)-one and 3-chloropropionyl chloride, the same procedure as in Reference Example 2 was followed, to yield the title compound as a colorless needle crystal having a melting point of 175° to 178° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05527800 |
| 出典データセット | uspto-grants-1996_06 |
| ORD ID | ord-3fb41dddd3f649798c7ec5da91331f3d |
| 出典メモ | uspto-grants-1996_06 |