反応式
[C:1]([CH2:4][C:5]1[CH:13]=[CH:12][CH:11]=[CH:10][C:6]=1[C:7]([OH:9])=O)(O)=O.[NH2:14][C:15]([CH3:19])([CH3:18])[CH2:16][SH:17].C([O-])(=O)C.[Na+]>ClC1C=CC=CC=1Cl>[CH3:18][C:15]1([CH3:19])[N:14]2[C:7](=[O:9])[C:6]3[CH:10]=[CH:11][CH:12]=[CH:13][C:5]=3[CH:4]=[C:1]2[S:17][CH2:16]1参加物
5
実験手順
By following the same procedure as in Example 49 using a mixture of 240 mg. of 2-carboxymethylbenzoic acid, 300 mg. of 2-amino-2-methylpropanethiol, 164 mg. of sodium acetate, and 5 ml. of o-dichlorobenzene, 120 mg. of 3,3-dimethyl-5-oxo-2,3-dihydro-5H-thiazolo[3,2-b]isoquinoline was obtained.
後処理
- additiona mixture of 240 mg
出典と根拠
- ORDレコード
- ord-64cfce68ca0c405c91b0742af24d77f8
- 出典データセット
- uspto-grants-1979_08
- 特許番号
- US04163844
関連ノート
読み込み中…