化工社化工社 化学情報印刷レポート · 研究参考用
Beta-Nitrostyrene → alpha-(Nitromethyl)benzyl diethyldithiocarbamate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Beta-Nitrostyrene | HCID 7626 | — |
| 反応物 | Diethylammonium diethylcarbamodithioate | HCID 2735004 | — |
| 溶媒 | Carbon Disulfide | HCID 6348 | — |
| 生成物 | alpha-(Nitromethyl)benzyl diethyldithiocarbamate | HCID 21324593 | — |
反応手順
As in Example 17, reaction of β-nitrostyrene with diethylammonium diethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)benzyl diethyldithiocarbamate melting at 81° C.-82.5° C. when recrystallized without heating from acetone-2-propanol solution.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04148795 |
| 出典データセット | uspto-grants-1979_04 |
| ORD ID | ord-021db1f139f940299dd9a715ed39cc5e |
| 出典メモ | uspto-grants-1979_04 |