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HRID26141

反应详情

EQUATION

反应方程式

HRID 26141 的结构方程式

REACTANTS

反应物

2
结构：O=[N+]([O-])C=Cc1ccccc1
HCID7626

beta-Nitrostyrene

C8H7NO2

结构：CCN(CC)C(=S)[S-].CC[NH2+]CC
HCID2735004

未命名化合物

PRODUCTS

生成物

1
结构：CCN(CC)C(=S)SC(C[N+](=O)[O-])c1ccccc1
HCID21324593

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：S=C=S
溶剂HCID6348

Carbon disulfide

CS2

PROCEDURE

实验过程

As in Example 17, reaction of β-nitrostyrene with diethylammonium diethyldithiocarbamate in the presence of carbon disulfide gave α-(nitromethyl)benzyl diethyldithiocarbamate melting at 81° C.-82.5° C. when recrystallized without heating from acetone-2-propanol solution.