Acetohydrazide → HCID 21315322、化合物

HRID 261798ノート

反応式

HRID 261798 の反応式
[CH2:1]([N:4]=[C:5]=[O:6])[CH:2]=[CH2:3].[C:7]([NH:10][NH2:11])(=[O:9])[CH3:8]>C1C=CC=CC=1>[C:7]([NH:10][NH:11][C:5]([NH:4][CH2:1][CH:2]=[CH2:3])=[O:6])(=[O:9])[CH3:8]

参加物

4

反応物 2

HCID 14039AcetohydrazideHCID 15123Allyl isocyanate

生成物 1

HCID 21315322HCID 21315322、化合物

試薬・触媒・溶媒 1

HCID 241Benzene溶媒

実験手順

Allyl isocyanate (25 g, 0.30 mol) was added slowly to a boiling solution of acethydrazide (22.2 g, 0.30 mol) in dry benzene (300 ml). The mixture was heated for 1 hour whereupon 2 layers formed. The benzene was then evaporated off and the residue triturated with ether to yield the title compound as a white solid. (m.p. 71°-74° C. ).

後処理

  1. temperatureThe mixture was heated for 1 hour whereupon 2 layers
  2. customformed
  3. customThe benzene was then evaporated off
  4. customthe residue triturated with ether

出典と根拠

ORDレコード
ord-773a273f5c404ff898f55b3702bd581b
出典データセット
uspto-grants-1979_05
特許番号
US04152442

反応ノート

読み込み中…