Water → HCID 20571322、化合物

HRID 261905

反応式

HRID 261905 の反応式
[CH3:1][O:2][CH2:3][CH2:4]O.[CH3:6][O:7][C:8](=[O:18])[C:9]1[CH:14]=[C:13]([Cl:15])[C:12]([OH:16])=[C:11]([Cl:17])[CH:10]=1.[OH-:19].[Na+].Br[CH2:22][C:23]1[C:28]([Br:29])=[C:27]([Br:30])[C:26]([Br:31])=[C:25]([CH2:32]Br)[C:24]=1[Br:34].[OH2:35]>>[C:8]([C:9]1[CH:10]=[C:11]([Cl:17])[C:12]([O:16][CH2:22][C:23]2[C:28]([Br:29])=[C:27]([Br:30])[C:26]([Br:31])=[C:25]([CH2:32][O:19][C:12]3[C:13]([Cl:15])=[CH:14][C:4]([C:3]([O:2][CH3:1])=[O:35])=[CH:10][C:11]=3[Cl:17])[C:24]=2[Br:34])=[C:13]([Cl:15])[CH:14]=1)([O:7][CH3:6])=[O:18]

参加物

6

反応物 5

HCID 962WaterHCID 80192-MethoxyethanolHCID 14798Sodium HydroxideHCID 76856Methyl 3,5-dichloro-4-hydroxybenzoateHCID 144191771,2,3,5-Tetrabromo-4,6-bis(bromomethyl)benzene

生成物 1

HCID 20571322HCID 20571322、化合物

実験手順

In a four-liter reaction vessel, 3 liters of methyl glycol (B.P. 122°-126° C.), 221 g (1 mole) of 3,5-dichloro-4-hydroxybenzoic acid methyl ester, 40 g (1 mole) of sodium hydroxide in 40 ml of water, and 289.8 g (0.5 mole) of 1,3-bis-(bromomethyl)-2,4,5,6-tetrabromobenzene were reacted and worked up in the manner described in Example 46.

後処理

  1. customwere reacted

出典と根拠

ORDレコード
ord-e26386e68cc4414b80148d386f0c134c
出典データセット
uspto-grants-1979_05
特許番号
US04152511

関連ノート

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