Hydrogen Bromide → 4-Benzylbenzyl bromide

HRID 262198ノート

反応式

HRID 262198 の反応式
C(C1C=CC(CO)=CC=1)C1C=CC=CC=1.Br.CO[C:19]1[CH:33]=[CH:32][C:22]([CH2:23][C:24]2[CH:31]=[CH:30][C:27]([CH2:28][Br:29])=[CH:26][CH:25]=2)=[CH:21][CH:20]=1>>[CH2:23]([C:24]1[CH:25]=[CH:26][C:27]([CH2:28][Br:29])=[CH:30][CH:31]=1)[C:22]1[CH:21]=[CH:20][CH:19]=[CH:33][CH:32]=1

参加物

4

反応物 3

HCID 260Hydrogen BromideHCID 5976144-(Phenylmethyl)benzenemethanolHCID 124638481-(Bromomethyl)-4-[(4-methoxyphenyl)methyl]benzene

生成物 1

HCID 100382674-Benzylbenzyl bromide

実験手順

4-Benzylbenzyl bromide was prepared from 20 g. of 4-benzylbenzyl alcohol [Maquin et al., Compt. rend. 234, 629-31, 1952] and hydrogen bromide according to the procedure of Example 1, part (e). An oil (25.7 g.) was obtained which was used directly in the next reaction.

後処理

  1. customAn oil (25.7 g.) was obtained which
  2. customwas used directly in the next reaction

出典と根拠

ORDレコード
ord-3396f1a26b9e40c2afefe39eeb1a8108
出典データセット
uspto-grants-1979_05
特許番号
US04153719

反応ノート

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