Acrylonitrile → 3-[(3-Hydroxypropyl)amino]propanenitrile

HRID 263172ノート

反応式

HRID 263172 の反応式
[NH2:1][CH2:2][CH2:3][CH2:4][OH:5].[C:6](#[N:9])[CH:7]=[CH2:8]>>[C:6]([CH2:7][CH2:8][NH:1][CH2:2][CH2:3][CH2:4][OH:5])#[N:9]

参加物

3

反応物 2

HCID 7855AcrylonitrileHCID 90863-Amino-1-propanol

生成物 1

HCID 135569403-[(3-Hydroxypropyl)amino]propanenitrile

実験手順

A solution of 75 g. (1 mole) of 3-aminopropanol is stirred while 54 g. (1 mole) of acrylonitrile is added dropwise. After being allowed to stand at room temperature for several hours and preferably overnight, the reaction mixture is concentrated under reduced pressure at 50° yielding 3-(2-cyanoethyl)aminopropanol.

後処理

  1. concentrationthe reaction mixture is concentrated under reduced pressure at 50°

出典と根拠

ORDレコード
ord-6c18ed7a1465480899fe070bc71a7c5b
出典データセット
uspto-grants-1979_05
特許番号
US04156693

反応ノート

読み込み中…