化工社化工社 化学情報印刷レポート · 研究参考用
2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid → Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-[6-Fluoro-2-methyl-3-[(4-methylsulfonylphenyl)methylidene]inden-1-yl]acetic acid | HCID 114866 | — |
| 反応物 | Sodium Methoxide | HCID 10942334 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | Sodium 5-fluoro-2-methyl-1-(rho-methylsulfonylbenzylidene)-3-indenylacetate | HCID 70149782 | — |
反応手順
5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetic acid (1.79 g.) in methanol (10 ml.) is added to a solution of sodium methoxide (0.27 g.) in methanol (5 ml.). The reaction mixture is stirred for 20 minutes and evaporated to dryness to yield sodium 5-fluoro-2-methyl-1-(ρ-methylsulfonylbenzylidene)-3-indenylacetate.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US05643959 |
| 出典データセット | uspto-grants-1997_07 |
| ORD ID | ord-cd04c875f5ec4961a8fe1d10a69de86b |
| 出典メモ | uspto-grants-1997_07 |