5,5'-Bi-2-benzofuran-1,1',3,3'-tetrone → Bpda tfmb

HRID 265912

反応式

HRID 265912 の反応式
[CH:1]1[C:6]([C:7]2[CH:12]=[CH:11][C:10]3[C:13]([O:15][C:16](=[O:17])[C:9]=3[CH:8]=2)=[O:14])=[CH:5][C:4]2[C:18]([O:20][C:21](=[O:22])[C:3]=2[CH:2]=1)=[O:19].[CH:23]1[C:28]([NH2:29])=[CH:27][C:26]([C:30]([F:33])([F:32])[F:31])=[C:25]([C:34]2[CH:39]=[CH:38][C:37]([NH2:40])=[CH:36][C:35]=2[C:41]([F:44])([F:43])[F:42])[CH:24]=1>CN1C(=O)CCC1>[CH:1]1[C:6]([C:7]2[CH:12]=[CH:11][C:10]3[C:13]([O:15][C:16](=[O:17])[C:9]=3[CH:8]=2)=[O:14])=[CH:5][C:4]2[C:18]([O:20][C:21](=[O:22])[C:3]=2[CH:2]=1)=[O:19].[CH:38]1[C:37]([NH2:40])=[CH:36][C:35]([C:41]([F:44])([F:42])[F:43])=[C:34]([C:25]2[CH:24]=[CH:23][C:28]([NH2:29])=[CH:27][C:26]=2[C:30]([F:31])([F:32])[F:33])[CH:39]=1

参加物

4

反応物 2

HCID 754945,5'-Bi-2-benzofuran-1,1',3,3'-tetroneHCID 629349(1,1'-Biphenyl)-4,4'-diamine, 2,2'-bis(trifluoromethyl)-

生成物 1

HCID 131720099Bpda tfmb

試薬・触媒・溶媒 1

HCID 13387N-methyl-2-pyrrolidone溶媒

実験手順

A solution of polyamic acid was prepared at room temperature by combining 6.893 grams of 6FDA, 1.518 grams of BPDA, 6.608 grams of TFMB and 61.1 grams of NMP with good mixing. The amic acid solution was diluted to 10.9% solids, then cast on a silicon wafer by spin coating, and imidized by a heat treatment up to a maximum temperature of 300° C. to produce a coating having a thickness of 2.1 microns. The refractive index was determined in the same manner as in Example 1 and is reported in Table I.

後処理

  1. customA solution of polyamic acid was prepared at room temperature
  2. customimidized by a heat treatment up to a maximum temperature of 300° C.
  3. customto produce a coating

出典と根拠

ORDレコード
ord-dbed9e972a19472fba1f3c23efa6faf6
出典データセット
uspto-grants-1997_07
特許番号
US05649045

関連ノート

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