Carbon Dioxide → Hydroquinone carbon dioxide

HRID 2665

反応式

HRID 2665 の反応式
[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].[C:9](=[O:11])=[O:10]>C(O)CC>[C:1]1([CH:8]=[CH:7][C:5]([OH:6])=[CH:4][CH:3]=1)[OH:2].[C:9](=[O:11])=[O:10]

参加物

4

反応物 2

HCID 280Carbon DioxideHCID 785Hydroquinone

生成物 1

HCID 86752301Hydroquinone carbon dioxide

試薬・触媒・溶媒 1

HCID 10311-Propanol溶媒

実験手順

Hydroquinone (30 g) was dissolved in n-propanol (70 ml) at 70° C. The hot solution was introduced into the high pressure autoclave. The solution was subjected to compressed carbon dioxide of 300 bar. The high pressure autoclave was kept for 2 h at 80° C. Then the solution was cooled down to room temperature within 5 days. The crystals were filtered off and washed 4 times with cold n-propanol (5 ml). The crystals were then dried in the drying cabinet at 70° C.

後処理

  1. additionThe hot solution was introduced into the high pressure autoclave
  2. filtrationThe crystals were filtered off
  3. washwashed 4 times with cold n-propanol (5 ml)
  4. customThe crystals were then dried in the drying cabinet at 70° C.

出典と根拠

ORDレコード
ord-598e5ea1d2164dab8e306d31809079d4
出典データセット
uspto-grants-1998_03
特許番号
US05730954

関連ノート

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