Urea → Urea neopentane

4 g urea were dissolved in 12 ml ethanol at 60° C. The solution was then placed in a high pressure autoclave and subjected to a neopentane pressure of 150 bar. The solution was cooled down from 60° C. to room temperature within 48 h. The solution with h/g crystals was removed from the autoclave, filtered and the h/g crystals were washed with 10 ml cold ethanol. The h/g complex crystals were dried in the vacuum cabinet at 60° C.

1. temperatureThe solution was cooled down from 60° C. to room temperature within 48 h
2. customThe solution with h/g crystals was removed from the autoclave
3. filtrationfiltered
4. washthe h/g crystals were washed with 10 ml cold ethanol
5. customThe h/g complex crystals were dried in the vacuum cabinet at 60° C.

ORDレコード

ord-73f99bd74f564708835c9ff95325d839

出典データセット

uspto-grants-1998_03

DOI

10.6084/m9.figshare.5104873.v1

特許番号

US05730954