Neopentane → Thiourea neopentane

4 g thiourea were dissolved in 20 ml ethanol at 60° C. The solution was then placed in a high pressure autoclave and subjected to a neopentane pressure of 150 bar. The solution was cooled down to room temperature within 60 h. The solution with h/g crystals was removed from the autoclave, filtered and the h/g crystals were washed with 10 ml cold ethanol. The h/g complex crystals were dried in the vacuum cabinet at 60° C.

1. customThe solution with h/g crystals was removed from the autoclave
2. filtrationfiltered
3. washthe h/g crystals were washed with 10 ml cold ethanol
4. customThe h/g complex crystals were dried in the vacuum cabinet at 60° C.

ORDレコード

ord-6524f1bde06c4fafba21ea58a8da26cd

出典データセット

uspto-grants-1998_03

DOI

10.6084/m9.figshare.5104873.v1

特許番号

US05730954