Hydrazine hydrate (1:1) → 5-Trifluoromethyl-2-aminobenzophenone hydrazone

HRID 267405ノート

反応式

HRID 267405 の反応式
[F:1][C:2]([F:19])([F:18])[C:3]1[CH:4]=[CH:5][C:6]([NH2:17])=[C:7]([CH:16]=1)[C:8]([C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1)=O.O.[NH2:21][NH2:22]>C(O)COCCO>[F:1][C:2]([F:19])([F:18])[C:3]1[CH:4]=[CH:5][C:6]([NH2:17])=[C:7]([CH:16]=1)[C:8](=[N:21][NH2:22])[C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1

参加物

4

反応物 2

HCID 24654Hydrazine hydrate (1:1)HCID 13014169(2-Amino-5-(trifluoromethyl)phenyl)(phenyl)methanone

生成物 1

HCID 867331125-Trifluoromethyl-2-aminobenzophenone hydrazone

試薬・触媒・溶媒 1

HCID 8117Diethylene Glycol溶媒

実験手順

In the manner given in Preparation 1, 5-(trifluoromethyl)-2-aminobenzophenone is refluxed with hydrazine hydrate in diethylene glycol to give 5-(trifluoromethyl)-2-aminobenzophenone hydrazone.

出典と根拠

ORDレコード
ord-38daa16c00da41a7ad4be40c09e21639
出典データセット
uspto-grants-1976_03
特許番号
US03941803

反応ノート

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