Pyrrolidine → HCID 68135941、化合物
反応式
[CH3:1][C:2]([NH:8][C:9](=[O:14])[CH2:10][CH2:11][O:12][CH3:13])([CH3:7])[CH2:3][C:4](=O)[CH3:5].[NH:15]1[CH2:19][CH2:18][CH2:17][CH2:16]1.[H][H]>[Pt]=O.CO>[CH3:1][C:2]([NH:8][C:9](=[O:14])[CH2:10][CH2:11][O:12][CH3:13])([CH3:7])[CH2:3][CH:4]([N:15]1[CH2:19][CH2:18][CH2:17][CH2:16]1)[CH3:5]参加物
6
実験手順
Following the procedure of Example 1, 20.1 grams (0.1 mole) of N-(1,1-dimethyl-3-oxobutyl)-3-methoxypropionamide is reacted with 10 grams (0.14 mole) of pyrrolidine in the presence of 0.3 gram of platinum oxide and 100 ml. of methanol. When hydrogen uptake has ceased, the methanol is stripped and the product, N-(1,1-dimethyl-3-pyrrolidylbutyl)-3-methoxypropionamide, is isolated as described in Example 1.
出典と根拠
- ORDレコード
- ord-c5552b5c0ef1424cbdf6541c6345d1df
- 出典データセット
- uspto-grants-1976_03
- 特許番号
- US03943114
反応ノート
読み込み中…