Vinyl ether → 2,2'-Dithenyl sulfide

反応式

C(O[CH:4]=[CH2:5])=C.[C:6]1([CH2:11][SH:12])[S:10][CH:9]=[CH:8][CH:7]=1>>[C:6]1([CH2:11][S:12][CH2:11][C:6]2[S:10][CH:5]=[CH:4][CH:7]=2)[S:10][CH:9]=[CH:8][CH:7]=1

参加物

反応物 2

HCID 8024Vinyl ether

HCID 80408Thenyl mercaptan

生成物 1

HCID 542107622,2'-Dithenyl sulfide

実験手順

f. Dithenyl sulfide was prepared by the same method as used for compound (1) b. (diethenyl ether) of Group X above, except that thenylmercaptan was used instead of thenyl alcohol. The product has a b.p. of 118°C./0.04 mm. Hg.

出典と根拠

ORDレコード: ord-b5b2d9c4b1314b0b96ded382154c946c
出典データセット: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US03943260

反応ノート

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