2-Ethylhexanol → Toluene 2,4-Diisocyanate

HRID 268150

反応式

HRID 268150 の反応式
[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][OH:5])[CH3:2].[CH3:10][C:11]1[CH:16]=[CH:15][C:14]([N:17]=[C:18]=[O:19])=[CH:13][C:12]=1[N:20]=[C:21]=[O:22].C(C(C)=O)CCC>>[NH2:17][C:18]([O:5][CH2:4][CH3:3])=[O:19].[CH2:1]([CH:3]([CH2:6][CH2:7][CH2:8][CH3:9])[CH2:4][OH:5])[CH3:2].[CH3:10][C:11]1[CH:16]=[CH:15][C:14]([N:17]=[C:18]=[O:19])=[CH:13][C:12]=1[N:20]=[C:21]=[O:22]

参加物

5

反応物 3

HCID 77202-EthylhexanolHCID 11443Toluene 2,4-DiisocyanateHCID 115832-Hexanone

生成物 2

HCID 11443Toluene 2,4-DiisocyanateHCID 879616842-Ethylhexanol monourethane

実験手順

A 2-ethylhexanol monourethane of 2,4-toluene diisocyanate sample was prepared by adding 651 parts of 2-ethylhexanol to an agitated mixture of 870 parts of 2,4-TDI and 100 parts methyl butyl ketone over approximately 3 hours, with external cooling to maintain the reaction temperature below 18° C. After addition was complete, the batch was agitated an additional 2 hours and stored under dry nitrogen for subsequent use.

後処理

  1. temperaturewith external cooling
  2. temperatureto maintain the reaction temperature below 18° C
  3. additionAfter addition

出典と根拠

ORDレコード
ord-915385be45e84c168c5487d71f9cf3c5
出典データセット
uspto-grants-1976_03
特許番号
US03947339

関連ノート

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