Borane → HCID 54525598、化合物
反応式
[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]([CH3:12])[C:10](=[O:13])[CH:9]3[CH2:14][CH2:15][CH2:16][N:8]3[C:7](=O)[C:6]=2[CH:18]=1.B>O1CCCC1>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]2[N:11]([CH3:12])[C:10](=[O:13])[CH:9]3[CH2:14][CH2:15][CH2:16][N:8]3[CH2:7][C:6]=2[CH:18]=1参加物
4
実験手順
If 7-chloro-1,2,3,11a-tetrahydro-10-methyl-5 H-pyrrolo[2,1-c] [1,4] benzodiazepin-5,11(10H)-dione (prepared as described in Example 1 from DL-proline and 5 -chloro-N-methylisatoic anhydride) is treated with 1M borane in tetrahydrofuran as described in Example 1, the above compound is obtained. The hydrochloride salt melts at 243°-245°C.
後処理
- customthe above compound is obtained
出典と根拠
- ORDレコード
- ord-d2a288af25a54d85b7fa4a3779b74cda
- 出典データセット
- uspto-grants-1976_03
- 特許番号
- US03947408
反応ノート
読み込み中…