2-Amino-4-chlorophenol → 2-Acetylamino-4-chlorophenol
反応式
[NH2:1][C:2]1[CH:7]=[C:6]([Cl:8])[CH:5]=[CH:4][C:3]=1[OH:9].[C:10](OC(=O)C)(=[O:12])[CH3:11]>CO>[Cl:8][C:6]1[CH:5]=[CH:4][C:3]([OH:9])=[C:2]([NH:1][C:10](=[O:12])[CH3:11])[CH:7]=1参加物
4
実験手順
To a suspension of 2-amino-4-chlorophenol (1.43 g, 10.0 mmol) in methanol was added acetic anhydride (0.945 mL, 10.0 mmol) and the reaction mixture was stirred at room temperature for 2 h. The volatiles were removed in vacuo to give the subtitled compound (1.5 g).
後処理
- customThe volatiles were removed in vacuo
出典と根拠
- ORDレコード
- ord-40c22dff81724e1d9b69e1626f222a07
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07449475B2
反応ノート
読み込み中…