反応式
[C:1]([C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([F:9])[CH:4]=1)#[CH:2].[Li]CCCC.[C:15]([C:19](OCC)=O)([F:18])([F:17])[F:16].B(F)(F)F.O(CC)CC.[NH2:33][NH2:34]>C1COCC1.C1C=CC=CC=1>[F:9][C:5]1[CH:4]=[C:3]([C:1]2[NH:34][N:33]=[C:19]([C:15]([F:18])([F:17])[F:16])[CH:2]=2)[CH:8]=[CH:7][CH:6]=1参加物
8
実験手順
Following protocol H, 1-Ethynyl-3-fluoro-benzene was treated with n-BuLi, CF3CO2Et and BF3—OEt2 in THF. Reaction with hydrazine in benzene under similar reaction conditions yielded title compound.
後処理
- customunder similar reaction conditions
出典と根拠
- ORDレコード
- ord-d8bdb191e76f452697277aaab9a78660
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07449576B1
関連ノート
読み込み中…