2-[(Thiazol-2-yl)methylthio]ethylamine → HCID 178433298、化合物

HRID 27096

反応式

HRID 27096 の反応式
[N+:1]([CH:4]=[C:5](SC)[NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])([O-:3])=[O:2].[NH2:19][CH2:20][CH2:21][S:22][CH2:23][C:24]1[S:25][CH:26]=[CH:27][N:28]=1>C(#N)C>[N+:1]([CH:4]=[C:5]([NH:6][CH2:7][CH2:8][S:9][CH2:10][C:11]1[NH:15][CH:14]=[N:13][C:12]=1[CH3:16])[NH:19][CH2:20][CH2:21][S:22][CH2:23][C:24]1[S:25][CH:26]=[CH:27][N:28]=1)([O-:3])=[O:2]

参加物

4

反応物 2

HCID 129234032-[(Thiazol-2-yl)methylthio]ethylamineHCID 178503826HCID 178503826、化合物

生成物 1

HCID 178433298HCID 178433298、化合物

試薬・触媒・溶媒 1

HCID 6342Acetonitrile溶媒

実験手順

Reaction of 1-nitro-2-methylthio-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]ethylene with an excess of 2-[(2-aminoethyl)thiomethyl]thiazole according to the procedure of Example 3, results in the production of 1-nitro-2-[2-((4-methyl-5-imidazolyl)methylthio)ethylamino]-2-[2-(2-thiazolylmethylthio)ethylamino]ethylene, m.p. 119°-120° (from acetonitrile).

出典と根拠

ORDレコード
ord-b63e13f868df4715906ad7213e09b6c0
出典データセット
uspto-grants-1980_09
特許番号
US04220652

関連ノート

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