Aniline → 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid
反応式
[CH2:1]=[C:2]1[CH2:7][C:6](=[O:8])[O:5][C:3]1=[O:4].[NH2:9][C:10]1[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1>CCl>[C:10]1([NH:9][C:6]([CH2:7][C:2](=[CH2:1])[C:3]([OH:5])=[O:4])=[O:8])[CH:15]=[CH:14][CH:13]=[CH:12][CH:11]=1参加物
4
実験手順
A solution of 2-methylenesuccinic anhydride (500 mg, 4.46 mmol) and aniline (0.4 mL, 4.46 mmol) in CH3Cl were shaken overnight. A precipitate formed, which was filtered off, washed with hexanes, and dried under vacuum to afford 2-[(N-phenylcarbamoyl)methyl]prop-2-enoic acid.
後処理
- customA precipitate formed
- filtrationwhich was filtered off
- washwashed with hexanes
- customdried under vacuum
出典と根拠
- ORDレコード
- ord-682c33e9511d4681b3e6095fa4659f39
- 出典データセット
- uspto-grants-2008_11
- 特許番号
- US07452889B2
反応ノート
読み込み中…