HCID 178479391、化合物 → HCID 178512583、化合物

HRID 27192

反応式

HRID 27192 の反応式
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]>[OH-].[Na+]>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH2:13])=[NH:12]

参加物

3

反応物 1

HCID 178479391HCID 178479391、化合物

生成物 1

HCID 178512583HCID 178512583、化合物

試薬・触媒・溶媒 1

HCID 14798Sodium Hydroxide溶媒

実験手順

The free base is prepared by dissolving 2,6-dichlorophenylguanidine hydrochloride in 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 2,6-dichlorophenylguanidine.

後処理

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

出典と根拠

ORDレコード
ord-a44b08c76d374b0796f109e5b67e825d
出典データセット
uspto-grants-1980_09
特許番号
US04220658

関連ノート

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