Sodium Hydroxide → HCID 178485099、化合物

HRID 27196

反応式

HRID 27196 の反応式
Cl.[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12].[OH-].[Na+]>>[Cl:2][C:3]1[CH:8]=[CH:7][CH:6]=[C:5]([Cl:9])[C:4]=1[NH:10][C:11]([NH:13][CH3:14])=[NH:12]

参加物

3

反応物 2

HCID 14798Sodium HydroxideHCID 178485100HCID 178485100、化合物

生成物 1

HCID 178485099HCID 178485099、化合物

実験手順

The free base is prepared by dissolving 1-(2,6-dichlorophenyl)-3-methylguanidine hydrochloride to 10% sodium hydroxide solution and extracting with ether. The ether is dried and evaporated to dryness to obtain 1-(2,6-dichlorophenyl)-3-methylguanidine.

後処理

  1. customThe free base is prepared
  2. extractionextracting with ether
  3. dry with materialThe ether is dried
  4. customevaporated to dryness

出典と根拠

ORDレコード
ord-833fa60e5f3742bea07aa37029c760bf
出典データセット
uspto-grants-1980_09
特許番号
US04220658

関連ノート

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