反応式
[OH2:1].[C:2]1([CH3:12])[CH:7]=[CH:6][C:5](S(O)(=O)=O)=[CH:4][CH:3]=1.[CH3:13][C:14](C)=[O:15]>>[O:1]=[C:2]([CH3:12])[CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:13][CH2:14][OH:15]参加物
3
実験手順
A solution containing 56.6 g of 8-oxononan-1-ol ethylene ketol (prepared in Example 22 B-5) in 210 ml acetone and 50 mg p-toluenesulfonic acid monohydrate was stirred at room temperature for about 15 to 17 hr. The acetone was removed in vacuo to yield the title compound having the following physical characteristics:
後処理
- customThe acetone was removed in vacuo
出典と根拠
- ORDレコード
- ord-693e33c552514efd8070df5fd9ba4b0a
- 出典データセット
- uspto-grants-1980_09
- 特許番号
- US04220795
関連ノート
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