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N-Ethyl cyclohexylamine → 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | N-Ethyl cyclohexylamine | HCID 21609 | — |
| 反応物 | 4-Chloro-3-nitrobenzophenone | HCID 41743 | — |
| 生成物 | 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone | HCID 23342778 | — |
反応手順
13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US04221739 |
| 出典データセット | uspto-grants-1980_09 |
| ORD ID | ord-84ea0d37cd7e4ceea09e7d996fe0f21e |
| 出典メモ | uspto-grants-1980_09 |