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HRID27378

反应详情

EQUATION

反应方程式

HRID 27378 的结构方程式

REACTANTS

反应物

2
结构：CCNC1CCCCC1
HCID21609

N-Ethyl cyclohexylamine

C8H17N

结构：O=C(c1ccccc1)c1ccc(Cl)c([N+](=O)[O-])c1
HCID41743

Benzophenone, 4-chloro-3-nitro-

C13H8ClNO3

PRODUCTS

生成物

1
结构：CCN(c1ccc(C(=O)c2ccccc2)cc1[N+](=O)[O-])C1CCCCC1
HCID23342778

未命名化合物

PROCEDURE

实验过程

13 g. of 3-nitro-4-chloro-benzophenone are reacted with 15 ml. of N-ethyl-N-cyclohexylamine as described in Example 2. The crude product is recrystallized from n-hexane to yield 15.3 g of pure, crystalline 3-nitro-4-(N-ethyl-N-cyclohexylamino)-benzophenone; m.p. 91.5°-92° C.

WORKUP

后处理

  1. customThe crude product is recrystallized from n-hexane