2-Methylbenzothiazole → HCID 22930888、化合物

HRID 275251

反応式

HRID 275251 の反応式
[CH3:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N:6]=1.[Br:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([OH:19])=[O:18]>>[Br-:11].[CH3:1][C:2]1[S:3][C:4]2[CH:10]=[CH:9][CH:8]=[CH:7][C:5]=2[N+:6]=1[CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][C:17]([OH:19])=[O:18]

参加物

3

反応物 2

HCID 84462-MethylbenzothiazoleHCID 202106-Bromohexanoic acid

生成物 1

HCID 22930888HCID 22930888、化合物収率 212.9%

反応条件

温度
120 °C

実験手順

2-methyl benzothiazole (19.5g, 0.1M) and 6-bromohexanoic acid (15.3g, 0.1M) were mixed and heated at 120° C. for 4 hours under continuous agitation. The resulting solid was broken up, ground with ether and then filtered. The filtrate was washed with more ether (250ml) to yield an off-white powder (57.5g).

後処理

  1. filtrationground with ether and then filtered
  2. washThe filtrate was washed with more ether (250ml)

出典と根拠

ORDレコード
ord-e9b9ffc8121942548db3ebc77f1545c8
出典データセット
uspto-grants-1995_02
特許番号
US05393654

関連ノート

読み込み中…