Hydrogen Bromide → HCID 18316762、化合物
反応式
[NH2:1][C:2]1[CH:10]=[CH:9][C:5]([CH2:6][CH2:7]O)=[CH:4][CH:3]=1.[BrH:11]>>[BrH:11].[Br:11][CH2:7][CH2:6][C:5]1[CH:9]=[CH:10][C:2]([NH2:1])=[CH:3][CH:4]=1参加物
3
実験手順
To 4-aminophenethyl alcohol (25 g) was added 48% hydrobromic acid (250 ml), and the mixture was heated under reflux for 4 hours with stirring. After cooling, collection of the resulting precipitates by filtration gave 4-(2-bromoethyl)aniline hydrobromide (30.3 g).
後処理
- temperaturethe mixture was heated
- temperatureunder reflux for 4 hours
- temperatureAfter cooling
- customcollection of the resulting
- customprecipitates by filtration
出典と根拠
- ORDレコード
- ord-027a6f8cf9374d9aa80d0ab52f08ffe0
- 出典データセット
- uspto-grants-2002_03
- 特許番号
- US06353025B1
反応ノート
読み込み中…