関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | Thionyl Chloride | HCID 24386 | — |
| 反応物 | (4-Phenoxyphenyl)methanol | HCID 826195 | — |
| 生成物 | 1-(Chloromethyl)-4-phenoxybenzene | HCID 520994 | 97.2% |
反応手順
Thionyl chloride (13.34 g) was added to 4.06 g of 4-phenoxybenzyl alcohol, and the mixture was stirred at 80° C. for 3.5 hours. After the completion of the concentration, the reaction mixture was extracted with ethyl acetate and with water. The organic layer was concentrated to give 4.31 g of 4-phenoxybenzyl chloride.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US06352985B1 |
|---|
| 出典データセット | uspto-grants-2002_03 |
|---|
| ORD ID | ord-e48630886bf3471b8d19ba088efbd56b |
|---|
| 出典メモ | uspto-grants-2002_03 |
|---|
