反应详情

温度

80 °C

Thionyl chloride (13.34 g) was added to 4.06 g of 4-phenoxybenzyl alcohol, and the mixture was stirred at 80° C. for 3.5 hours. After the completion of the concentration, the reaction mixture was extracted with ethyl acetate and with water. The organic layer was concentrated to give 4.31 g of 4-phenoxybenzyl chloride.

1. concentrationAfter the completion of the concentration
2. extractionthe reaction mixture was extracted with ethyl acetate and with water
3. concentrationThe organic layer was concentrated