Ethanolamine → HCID 18316365、化合物

HRID 276427

反応式

[CH:1]1([CH2:13]O)[CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.C1(CBr)CCCCCCCCCCC1.[OH:29][CH2:30][CH2:31][NH2:32]>>[OH:29][CH2:30][CH2:31][NH:32][CH2:13][CH:1]1[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12]1

参加物

反応物 3

HCID 700Ethanolamine

HCID 74686Cyclododecanemethanol

HCID 18316415HCID 18316415、化合物

生成物 1

HCID 18316365HCID 18316365、化合物

実験手順

Methyl cyclododecanecarboxylate was reduced according to Method B2b, Step 1 to give cyclododecylmethanol. The alcohol was converted to cyclododecylmethylbromide according to Method B2b, Step 2. The halide was reacted with 2-hydroxyethylamine according to Method B2b, Step 3 to give N-(2-hydroxyethyl)-N-(cyclododecylmethyl)amine. The alcohol was reacted with SOCl2 according to Method B7a to give N-(2-chloroethyl)-N-(cyclododecylmethyl)ammonium chloride. The chloroethylamine was reacted with 2-methyl-4-nitrophenyl isothiocyanate according to Method C1a to give 2-(2-methyl-4-nitrophenylimino)-3-(cyclododecylmethyl)-1,3 -thiazolidine.

出典と根拠

ORDレコード: ord-981e06a11c21447db0d13bd451d53b47
出典データセット: uspto-grants-2002_03
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US06353006B1

反応式

参加物

反応物 3

生成物 1

実験手順

出典と根拠

関連ノート