1-Fluoro-4-methoxy-2-vinylbenzene → 2-Ethyl-1-fluoro-4-methoxybenzene
反応式
[CH:1]([C:3]1[CH:4]=[C:5]([O:10][CH3:11])[CH:6]=[CH:7][C:8]=1[F:9])=[CH2:2]>C(O)C.[Pd]>[CH2:1]([C:3]1[CH:4]=[C:5]([O:10][CH3:11])[CH:6]=[CH:7][C:8]=1[F:9])[CH3:2]参加物
4
実験手順
To a solution of 9 g of 3-ethenyl-4-fluoroanisole in 200 ml of ethanol was added 0.9 g of palladium/carbon. The resulting mixture was stirred under hydrogen atmosphere overnight, and filtered through Celite. The filtrate was evaporated, and the resulting residue was subjected to silica gel column chromatography (developer: 50% ethyl acetate/n-hexane) to give 7.0 g of the title compound as a colorless oil.
後処理
- filtrationfiltered through Celite
- customThe filtrate was evaporated
出典と根拠
- ORDレコード
- ord-62a33c29d8374648932eba48a27d2fd2
- 出典データセット
- uspto-grants-2002_03
- 特許番号
- US06358995B1
反応ノート
読み込み中…