Water → Barium Tridecanephosphonate

HRID 27835

反応式

HRID 27835 の反応式
[Na+].[Na+].[CH2:3]([P:16](=[O:19])([O-:18])[O-:17])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].O.[Cl-].[Ba+2:22].[Cl-]>C(O)C>[CH2:3]([P:16]([O-:19])(=[O:17])[O-:18])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH3:15].[Ba+2:22]

参加物

5

反応物 3

HCID 962WaterHCID 5360350Barium(2+) dichlorideHCID 88784368HCID 88784368、化合物

生成物 1

HCID 23340094Barium Tridecanephosphonate収率 96.3%

試薬・触媒・溶媒 1

HCID 702Ethanol溶媒

実験手順

Tridecylphosphonic acid disodium salt 123 g (0.4 mole), distilled water 500 ml and ethanol 30 ml were charged into a reaction flask and dissolved by stirring at room temperature. To this solution, 20% barium chloride aq. solution 416 g (0.4 mole) was added and allowed to react for one hour at room temperature. The compound precipitated was filtered off, repeatedly washed with water until free of sodium chloride and dried to obtain 154 g of white powder.

後処理

  1. additionwere charged into a reaction flask
  2. dissolutiondissolved
  3. customto react for one hour at room temperature
  4. customThe compound precipitated
  5. filtrationwas filtered off
  6. washrepeatedly washed with water until free of sodium chloride
  7. customdried

出典と根拠

ORDレコード
ord-acf0677b27be4cc5b0219f09973a1e85
出典データセット
uspto-grants-1980_09
特許番号
US04224203

関連ノート

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