反応式
Cl.[OH:2][CH2:3][C:4]1[N:5]=[CH:6][NH:7][CH:8]=1.[CH:9]([O:11][CH2:12][CH3:13])=[CH2:10].C1(C)C=CC(S(O)(=O)=O)=CC=1>CN(C)C=O>[CH2:9]([O:11][CH:12]([O:2][CH2:3][C:4]1[N:5]=[CH:6][NH:7][CH:8]=1)[CH3:13])[CH3:10]参加物
5
実験手順
To a flask containing 4 gms 4-hydroxymethyl imidazole hydrochloride in 30 ml dimethylformamide add 3.1 ml vinylethyl ether and 50 mg paratoluene sulfonic acid. Stir for 11/2 hours until the reaction is complete. Extract from saturated K2CO3 /NaCl with ethylacetate to obtain 1-ethoxy-1-(imidazol-4-yl)methoxy ethane.
後処理
- extractionExtract from saturated K2CO3 /NaCl with ethylacetate
出典と根拠
- ORDレコード
- ord-66bf058a84f94f76b34dcf0fdc9167ee
- 出典データセット
- uspto-grants-1986_05
- 特許番号
- US04587241
関連ノート
読み込み中…