HCID 178497871、化合物 → methyl 3-(5-methyl-1H-[1,2,4]triazol-3-yl)-benzoate
反応式
[NH:1]=[C:2]([NH:4][NH:5][C:6]([C:8]1[CH:9]=[C:10]([CH:15]=[CH:16][CH:17]=1)[C:11]([O:13][CH3:14])=[O:12])=O)[CH3:3]>C(Cl)(Cl)Cl>[CH3:3][C:2]1[NH:4][N:5]=[C:6]([C:8]2[CH:9]=[C:10]([CH:15]=[CH:16][CH:17]=2)[C:11]([O:13][CH3:14])=[O:12])[N:1]=1参加物
3
実験手順
8.10 g (34.4 mmol) methyl 3-[N′-(1-imino-ethyl)-hydrazinocarbonyl]-benzoate are heated to 180° C. for 30 minutes. 80 mL chloroform are added to the solid obtained after cooling. The suspension is filtered and the product is dried. White solid.
後処理
- customobtained
- temperatureafter cooling
- filtrationThe suspension is filtered
- customthe product is dried
出典と根拠
- ORDレコード
- ord-4c1cda77f3b54753bc080c7c186804f4
- 出典データセット
- uspto-grants-2008_09
- 特許番号
- US07423036B2
反応ノート
読み込み中…