Hydrazine hydrate (1:1) → 7-methoxy-4-(3-methoxyphenyl)-2H-phthalazin-1-one

反応式

[CH3:1][O:2][C:3]1[CH:4]=[CH:5][C:6]([C:12](=O)[C:13]2[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[CH:14]=2)=[C:7]([CH:11]=1)[C:8](O)=[O:9].O.[NH2:23][NH2:24]>>[CH3:1][O:2][C:3]1[CH:11]=[C:7]2[C:6]([C:12]([C:13]3[CH:18]=[CH:17][CH:16]=[C:15]([O:19][CH3:20])[CH:14]=3)=[N:23][NH:24][C:8]2=[O:9])=[CH:5][CH:4]=1

参加物

反応物 2

HCID 24654Hydrazine hydrate (1:1)

HCID 3340815-Methoxy-2-(3-methoxybenzoyl)benzoic acid

生成物 1

HCID 692114497-methoxy-4-(3-methoxyphenyl)-2H-phthalazin-1-one

実験手順

This compound is obtained according to the procedure described in 1.2. by reacting unpurified 5-methoxy-2-(3-methoxybenzoyl)benzoic acid with hydrazine hydrate.

後処理

customThis compound is obtained

出典と根拠

ORDレコード: ord-da302e3ac43d45bd9526cd2ae653a4d6
出典データセット: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07423030B2

反応ノート

読み込み中…