Phenylacetyl chloride → 3,5-Dimethoxy-2-(phenylacetyl)benzoic acid

HRID 29966

反応式

HRID 29966 の反応式
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([O:8]C)=[O:7].[C:15]1([CH2:21][C:22](Cl)=[O:23])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH3:1][O:2][C:3]1[C:4]([C:22](=[O:23])[CH2:21][C:15]2[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=2)=[C:5]([CH:10]=[C:11]([O:13][CH3:14])[CH:12]=1)[C:6]([OH:8])=[O:7]

参加物

3

反応物 2

HCID 7679Phenylacetyl chlorideHCID 75074Methyl 3,5-Dimethoxybenzoate

生成物 1

HCID 692138893,5-Dimethoxy-2-(phenylacetyl)benzoic acid

実験手順

This compound is synthesized by reacting methyl 3,5-dimethoxybenzoate with phenylacetyl chloride via the Friedel-Crafts reaction, followed by saponification of the ester obtained, according to the method described in 2.1. It is used in crude form in the following reaction.

後処理

  1. customThis compound is synthesized
  2. customvia the Friedel-Crafts reaction
  3. customobtained
  4. customin the following reaction

出典と根拠

ORDレコード
ord-f474b4227e984e3b8f420708e210bfb8
出典データセット
uspto-grants-2008_09
特許番号
US07423030B2

関連ノート

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