Hydrazine hydrate (1:1) → 4-cyclopentyl-7-methoxy-2H-phthalazin-1-one

反応式

[CH:1]1([C:6]([C:8]2[CH:16]=[CH:15][C:14]([O:17][CH3:18])=[CH:13][C:9]=2[C:10](O)=[O:11])=O)[CH2:5][CH2:4][CH2:3][CH2:2]1.O.[NH2:20][NH2:21]>>[CH:1]1([C:6]2[C:8]3[C:9](=[CH:13][C:14]([O:17][CH3:18])=[CH:15][CH:16]=3)[C:10](=[O:11])[NH:21][N:20]=2)[CH2:5][CH2:4][CH2:3][CH2:2]1

参加物

反応物 2

HCID 24654Hydrazine hydrate (1:1)

HCID 692118112-Cyclopentanecarbonyl-5-methoxybenzoic acid

生成物 1

HCID 692139674-cyclopentyl-7-methoxy-2H-phthalazin-1-one

実験手順

This compound is obtained according to the procedure described in 1.2. by reacting unpurified 2-cyclopentanecarbonyl-5-methoxybenzoic acid with hydrazine hydrate.

後処理

customThis compound is obtained

出典と根拠

ORDレコード: ord-9c2d7c52fe0d49f3bc8f0d46a18bd774
出典データセット: uspto-grants-2008_09
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US07423030B2

反応ノート

読み込み中…