N~1~-(Pyridin-2-yl)ethane-1,2-diamine → 2-(2-Aminoethylamino)-5-nitropyridine

HRID 31853

反応式

HRID 31853 の反応式
NCCNC1N=CC=CC=1.ClC1C=C(Cl)C=CC=1C1C(C2NC=CN=2)=CN=C([NH:30][CH2:31][CH2:32][NH:33][C:34]2[CH:39]=[CH:38][C:37]([N+:40]([O-:42])=[O:41])=[CH:36][N:35]=2)N=1>N1C=CC=CC=1>[NH2:30][CH2:31][CH2:32][NH:33][C:34]1[CH:39]=[CH:38][C:37]([N+:40]([O-:42])=[O:41])=[CH:36][N:35]=1

参加物

4

反応物 2

HCID 410428N~1~-(Pyridin-2-yl)ethane-1,2-diamineHCID 9847557Chir-98023

生成物 1

HCID 1224252-(2-Aminoethylamino)-5-nitropyridine

試薬・触媒・溶媒 1

HCID 1049Pyridine溶媒

実験手順

The preparation of the material 6-[(2-aminoethyl)amino]pyridine with various substitutents on the pyridine can be found in the precedures for the preparation of [4-(2,4-dichlorophenyl)-5-imidazol-2-ylpyrimidin-2-yl]{2-[(5-nitro(2-pyridyl))amino]ethyl}amine, Example 74, and its analogues.

出典と根拠

ORDレコード
ord-ca90443a31224026b610bfc2ae112ae7
出典データセット
uspto-grants-2008_09
特許番号
US07425557B2

関連ノート

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