Sodium Sulfite → (4-Cyanophenyl)methanesulfonyl chloride
反応式
Br[CH2:2][C:3]1[CH:10]=[CH:9][C:6]([C:7]#[N:8])=[CH:5][CH:4]=1.[S:11]([O-:14])([O-])=[O:12].[Na+].[Na+].P(Cl)(Cl)(Cl)(Cl)[Cl:18]>>[C:7]([C:6]1[CH:9]=[CH:10][C:3]([CH2:2][S:11]([Cl:18])(=[O:14])=[O:12])=[CH:4][CH:5]=1)#[N:8]参加物
4
実験手順
4-Bromomethylbenzonitrile was reacted with sodium sulphite followed by phosphorus pentachloride to give 4-cyanobenzylsulphonyl chloride which was reacted with pentylamine in a similar manner to N14 to give the title compound.
出典と根拠
- ORDレコード
- ord-1890100223a64e3892700b891b31da93
- 出典データセット
- uspto-grants-2001_04
- 特許番号
- US06215001B1
反応ノート
読み込み中…