Methyl iodide → 1-N-methyl-4-(2-dimethylaminobenzylthio)-5,5-dimethyl-3-imidazolin-2-one
反応式
[CH3:1][N:2]([CH3:19])[C:3]1[CH:18]=[CH:17][CH:16]=[CH:15][C:4]=1[CH2:5][S:6][C:7]1[C:11]([CH3:13])([CH3:12])[NH:10][C:9](=[O:14])[N:8]=1.[CH3:20]I>>[CH3:20][N:10]1[C:11]([CH3:13])([CH3:12])[C:7]([S:6][CH2:5][C:4]2[CH:15]=[CH:16][CH:17]=[CH:18][C:3]=2[N:2]([CH3:1])[CH3:19])=[N:8][C:9]1=[O:14]参加物
3
実験手順
Initially, 0.5 g of 4-(2-dimethylaminobenzylthio)-5,5-dimethyl-3-imidazolin-2-one was reacted with 1 mL of methyl iodide following the procedure used in Example 35. The desired compound was obtained in the form of a syrup. The yield of this compound was 0.43 g with a yield ratio of 81.9%. A result of a 1 H-NMR analysis of the compound is as follows:
出典と根拠
- ORDレコード
- ord-963943015c7a4df68483236ac94750d2
- 出典データセット
- uspto-grants-1998_03
- 特許番号
- US05733922
反応ノート
読み込み中…