化工社化工社 化学情報印刷レポート · 研究参考用
1-Methyluracil → HCID 178432306、化合物
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 1-Methyluracil | HCID 12009 | — |
| 反応物 | (+/-)-7-Chloro-1-((imidazol-4-yl)ethyl)-2-methyl-4h-benzo[5,6]cyclohepta[1,2-d]imidazol-4-ol | HCID 178432308 | — |
| 生成物 | HCID 178432306 | HCID 178432306 | — |
反応手順
The subtitle product was prepared from the product of step (ii) and 1-methyluracil (0.36 g) according to the method of example 42 step (iv). Purification was by biotage chromatography on silica eluting with 5% methanol in dichloromethane with 1% 0.880 ammonia present to give a white solid.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06218376B1 |
| 出典データセット | uspto-grants-2001_04 |
| ORD ID | ord-83fd2bfa2f15441692957c68e4a50d22 |
| 出典メモ | uspto-grants-2001_04 |