2-Methoxyaniline → N-(2-Methoxyphenyl)benzeneethanamine
反応式
[CH3:1][O:2][C:3]1[C:4]([NH2:9])=[CH:5][CH:6]=[CH:7][CH:8]=1.[CH2:10]=[CH:11][C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>C(OCC)(=O)C.CCCCCC>[C:12]1([CH2:11][CH2:10][NH:9][C:4]2[CH:5]=[CH:6][CH:7]=[CH:8][C:3]=2[O:2][CH3:1])[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1参加物
4
実験手順
According to GWM, 0.011 mol (=1.25 ml) of o-anisidine and 0.011 mol (=1.25 ml) of styrene are reacted with one another. The product is isolated by column chromatography using ethyl acetate/n-hexane (1:5) as eluent, the product N-(2-phenylethyl)-(o-methoxy)aniline being obtained as a slightly pink liquid.
後処理
- customare reacted with one another
- customThe product is isolated by column chromatography
出典と根拠
- ORDレコード
- ord-f7aa953ef03b44a78e978fee00d53d46
- 出典データセット
- uspto-grants-2001_04
- 特許番号
- US06222073B1
反応ノート
読み込み中…