Sodium Hydroxide → HCID 23718315、化合物

HRID 326786ノート

反応式

HRID 326786 の反応式
[CH2:1]([CH:3]([CH2:13][CH3:14])[C:4]([NH:6][CH2:7][C:8]([O:10]CC)=[O:9])=[O:5])[CH3:2].[OH-].[Na+:16]>CO>[CH2:13]([CH:3]([CH2:1][CH3:2])[C:4]([NH:6][CH2:7][C:8]([O-:10])=[O:9])=[O:5])[CH3:14].[Na+:16]

参加物

4

反応物 2

HCID 14798Sodium HydroxideHCID 2268387Ethyl 2-(2-ethylbutanoylamino)acetate

生成物 1

HCID 23718315HCID 23718315、化合物

試薬・触媒・溶媒 1

HCID 887Methanol溶媒

実験手順

To a solution of ethyl N-(2-ethylbutyryl)glycinate (33.73 g) in 100 mL of methanol was added 167.6 mL of 1N sodium hydroxide, and the solution stirred for 1.5 hr. Solvents were evaporated in vacuo, and then fresh methanol was added and evaporated to give 32.6 g of a pale yellow oil.

後処理

  1. customSolvents were evaporated in vacuo
  2. additionfresh methanol was added
  3. customevaporated

出典と根拠

ORDレコード
ord-4e69deb7f80a40ca802f059a16d2cd57
出典データセット
uspto-grants-1993_12
特許番号
US05270331

反応ノート

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